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Removing the valve means that it's contaminated as far as oxygen is concerned, right?
It seems to me that they could have declined to fill it, but I'd say they owe you the cost of returning it to the original condition.
No matter what the industry, I don't believe that any business has the right to damage your property - even in the noble goal of 'safety' - unless there is a legal mandate/requirement for them to do so. Otherwise, they should be allowed to turn down your business but that's it, IMO...
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